Instrumental Data for Drug Analysis - 6 Volume Set

Instrumental Data for Drug Analysis

The authors and publisher have made every effort to assure the accuracy of the information in this book; however, they cannot be responsible for errors in publication or for any consequences arising from the use of the data published in INSTRUMENTAL DATA FOR DRUG ANALYSIS, THIRD EDITION.

Instrumental Data for Drug Analysis Third Edition Volume 4 Terry Mills III, James Conrad Roberson, Christian C. Matchett, Mathew J. Simon, Mark D. Burns, and Robert J. Ollis Jr.

Boca Raton London New York

A CRC title, part of the Taylor & Francis imprint, a member of the Taylor & Francis Group, the academic division of T&F Informa plc.

Published in 2006 by CRC Press Taylor & Francis Group 6000 Broken Sound Parkway NW, Suite 300 Boca Raton, FL 33487-2742 © 2006 by Taylor & Francis Group, LLC CRC Press is an imprint of Taylor & Francis Group No claim to original U.S. Government works Printed in the United States of America on acid-free paper 10 9 8 7 6 5 4 3 2 1 International Standard Book Number-10: 0-8493-1974-9 (Hardcover) International Standard Book Number-13: 978-0-8493-1974-7 (Hardcover) Library of Congress Card Number 2005048542 This book contains information obtained from authentic and highly regarded sources. Reprinted material is quoted with permission, and sources are indicated. A wide variety of references are listed. Reasonable efforts have been made to publish reliable data and information, but the author and the publisher cannot assume responsibility for the validity of all materials or for the consequences of their use. No part of this book may be reprinted, reproduced, transmitted, or utilized in any form by any electronic, mechanical, or other means, now known or hereafter invented, including photocopying, microfilming, and recording, or in any information storage or retrieval system, without written permission from the publishers. For permission to photocopy or use material electronically from this work, please access www.copyright.com (http://www.copyright.com/) or contact the Copyright Clearance Center, Inc. (CCC) 222 Rosewood Drive, Danvers, MA 01923, 978-750-8400. CCC is a not-for-profit organization that provides licenses and registration for a variety of users. For organizations that have been granted a photocopy license by the CCC, a separate system of payment has been arranged. Trademark Notice: Product or corporate names may be trademarks or registered trademarks, and are used only for identification and explanation without intent to infringe. Library of Congress Cataloging-in-Publication Data Instrumental data for drug analysis / by Terry Mills, III … [et al.]. – 3rd ed. p. cm. Includes index. Previous ed.: Instrumental data for drug analysis / by Terry Mills. Boca Raton : CRC Press 1993-1996. ISBN 0-8493-1974-9 (alk. paper) Drugs – Analysis – Standards. 2. Drugs – Spectra – Standards. 3. Instrumental analysis – Standards. I. Mills, Terry. II. Mills, Terry. Instrumental data for drug analysis. RS189.M54 2005 615’.1901 – dc22

2005048542

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Table of Contents VOLUME 1 PREFACE ................................................................................................................................................................vii ACKNOWLEDGMENTS.........................................................................................................................................ix INTRODUCTION ................................................................................................................................................... xi DRUG DATA Acebutolol – Dapsone .........................................................................................................................2

VOLUME 2 DRUG DATA Dauromycin – Indigotin Disulfonate...........................................................................................................816

VOLUME 3 DRUG DATA Indole-3-Acetic Acid – Phendimetrazine ..................................................................................................1638

VOLUME 4 DRUG DATA Phenelzine – Zoxazolamine .......................................................................................................................2454

VOLUME 5 RAMAN SPECTRA DATA ................................................................................................................................3279 MASS SPECTRA OF PESTICIDES ..................................................................................................................3691 MASS SPECTRA OF DERIVATIZED DRUGS................................................................................................3803 GAS CHROMATOGRAPHY/INFRARED SPECTRA OF DRUGS.................................................................3949

VOLUME 6 APPENDIX A: Standard KBr Infrared Spectra and Standard NMR Solvent Spectra ......................................4177 APPENDIX B: Supplemental Infrared Spectra ..................................................................................................4185 APPENDIX C: Supplemental NMR Spectra......................................................................................................4267 APPENDIX D: Ultraviolet Absorption Maxima ................................................................................................4293 APPENDIX E: Infrared Index.............................................................................................................................4371 APPENDIX F: Mass Spectra Indices of Drugs..................................................................................................4409 APPENDIX G: Mass Spectra Indices of Pesticides ...........................................................................................4461 APPENDIX H: Molecular Formula Index..........................................................................................................4473 APPENDIX I: Gas Chromatographic Data .......................................................................................................4509 INDEX TO SPECIFIC COMPOUNDS ..............................................................................................................4529

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2904

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2905

2906

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2907

2908

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2909

2910

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2911

2912

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2913

2914

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2915

2916

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2917

2918

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2919

2920

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2921

2922

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2923

2924

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2925

2926

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2927

2928

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2929

2930

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2931

2932

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2933

2934

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2935

2936

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2937

2938

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2939

2940

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2941

2942

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2943

2944

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2945

2946

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2947

2948

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2949

2950

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2951

2952

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2953

2954

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2955

2956

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2957

2958

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2959

2960

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2961

2962

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2963

2964

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2965

2966

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2967

2968

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2969

2970

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2971

2972

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2973

2974

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2975

2976

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2977

2978

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2979

2980

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2981

2982

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2983

2984

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2985

2986

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2987

2988

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2989

2990

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2991

2992

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2993

2994

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2995

2996

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2997

2998

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

2999

3000

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3001

3002

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3003

3004

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3005

3006

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3007

3008

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3009

3010

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3011

3012

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3013

3014

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3015

3016

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3017

3018

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3019

3020

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3021

3022

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3023

3024

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3025

3026

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3027

3028

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3029

3030

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3031

3032

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3033

3034

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3035

3036

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3037

3038

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3039

3040

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3041

3042

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3043

3044

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3045

3046

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3047

3048

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3049

3050

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3051

3052

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3053

3054

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3055

3056

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3057

3058

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3059

3060

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3061

3062

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3063

3064

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3065

3066

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3067

3068

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3069

3070

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3071

3072

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3073

3074

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3075

3076

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3077

3078

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3079

3080

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3081

3082

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3083

3084

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3085

3086

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3087

3088

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3089

3090

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3091

3092

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3093

3094

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3095

3096

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3097

3098

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3099

3100

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3101

3102

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3103

3104

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3105

3106

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3107

3108

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3109

3110

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3111

3112

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3113

3114

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3115

3116

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3117

3118

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3119

3120

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3121

3122

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3123

3124

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3125

3126

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3127

3128

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3129

3130

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3131

3132

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3133

3134

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3135

3136

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3137

3138

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3139

3140

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3141

3142

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3143

3144

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3145

3146

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3147

3148

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3149

3150

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3151

3152

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3153

3154

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3155

3156

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3157

3158

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3159

3160

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3161

3162

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3163

3164

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3165

3166

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3167

3168

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3169

3170

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3171

3172

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3173

3174

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3175

3176

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3177

3178

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3179

3180

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3181

3182

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3183

3184

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3185

3186

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3187

3188

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3189

3190

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3191

3192

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3193

3194

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3195

3196

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3197

3198

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3199

3200

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3201

3202

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3203

3204

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3205

3206

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3207

3208

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3209

3210

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3211

3212

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3213

3214

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3215

3216

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3217

3218

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3219

3220

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3221

3222

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3223

3224

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3225

3226

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3227

3228

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3229

3230

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3231

3232

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3233

3234

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3235

3236

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3237

3238

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3239

3240

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3241

3242

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3243

3244

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3245

3246

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3247

3248

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3249

3250

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3251

3252

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3253

3254

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3255

3256

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3257

3258

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3259

3260

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3261

3262

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3263

3264

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3265

3266

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3267

3268

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3269

3270

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3271

3272

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3273

3274

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3275

3276

Instrumental Data for Drug Analysis

Volume 4: Phenelzine – Zoxazolamine

3277